From monomer to micelle: a facile approach to the multi-step synthesis of block copolymers <i>via</i> inline purification

Voorter, Pieter-Jan; Ammini, Gayathri Dev; Buckinx, Axel; Dai, Jin; Subramanian, Priya; Kumar, Anil; Cameron, Neil R.; Junkers, Thomas

doi:10.1039/d3sc01819a

Chem. Sci.

2023

DOI: 10.1039/d3sc01819a

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From monomer to micelle: a facile approach to the multi-step synthesis of block copolymers via inline purification

Pieter-Jan Voorter

Gayathri Dev Ammini

Axel Buckinx

et al.

Abstract: A one-pass continuous flow strategy to form block copolymer nanoaggregates directly from monomers is presented. A key development towards such sophisticated continuous flow setup is a significant improvement in continuous...

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2024

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Cited by 3 publications

References 33 publications

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Streamlined Formation and Manipulation of Charged Polymersomes

Lai,

Wong,

Stenzel

2024

Small

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Charged polymersomes are attractive for advanced material applications due to their versatile encapsulation capabilities and charge‐induced functionality. Although desirable, the pH‐sensitivity of charged block copolymers adds complexity to its self‐assembly process, making it challenging to produce charged polymersomes in a reliable manner. In this work, a flow approach to control and strike a delicate balance between solvent composition and pH for self‐assembly is used. This allows for the identification of a phase window to reliably produce of charged polymersomes. The utility of this approach to streamline downstream processes, such as morphological transformation or in‐line purification is further demonstrated. As proof‐of‐concept, it is shown that the processed polymersomes can be used for surface modifications facilitated by charge complexation.

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Streamlined Formation and Manipulation of Charged Polymersomes

Lai,

Wong,

Stenzel

2024

Small

View full text Add to dashboard Cite

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CTCOSY-JRES: A high-resolution three-dimensional NMR method for unveiling J-couplings

Lin,

Chen,

Huang

et al. 2024

Journal of Magnetic Resonance

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Accelerated Continuous Flow Depolymerization of Poly(Methyl Methacrylate)

Jäger,

Ammini,

Voorter

et al. 2024

J. Am. Chem. Soc.

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From monomer to micelle: a facile approach to the multi-step synthesis of block copolymers via inline purification

Abstract: A one-pass continuous flow strategy to form block copolymer nanoaggregates directly from monomers is presented. A key development towards such sophisticated continuous flow setup is a significant improvement in continuous...

Cited by 3 publications

References 33 publications

Streamlined Formation and Manipulation of Charged Polymersomes

Streamlined Formation and Manipulation of Charged Polymersomes

CTCOSY-JRES: A high-resolution three-dimensional NMR method for unveiling J-couplings

Accelerated Continuous Flow Depolymerization of Poly(Methyl Methacrylate)

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