Full assignments of the ¹H and ¹³C NMR spectra of sodium fusidate in organic and aqueous media

Abstract

The 1H and 13C nuclear magnetic resonance spectra of sodium fusidate in methanol‐d4 and in D2O have been assigned using a range of one‐ and two‐dimensional NMR techniques.

Structural characterization of triorganotin(IV) complexes with sodium fusidate and DFT calculations

“…R 3 SnCl (R = Me, Bu, Ph) used in the syntheses were Fluka-Riedel-de Haën (Sigma-Aldrich Company, St. Louis, MO, USA) products, while the free fusidic acid sodium salt ligand [28] (Fig. 1) was a Sigma-Aldrich Co. product.…”

“…Chemical structure of steroid sodium fusidate, with the numbering scheme referred to the NMR assignments (according to Ref. [28]). 22 MHz on a Bruker Avance II DMX 400 MHz (9.40 T) spectrometer (Bruker BioSpin GmbH, Rheinstetten, Germany).…”