“…The peak fitting of C 1s and N 1s regions’ deconvolution spectra is used to evaluate the detailed chemical bonds of the fiber surface (displayed in Figure b–e, Table S2 and Figure S2). For the C 1s spectra, the original three peaks are assigned to C–C (284.6 eV), C–N (285.7 eV), and C–O (286 eV) of the de-sized CF. ,,, After co-deposition of TA/POSS on the fiber surface, four new peaks are observed, which can be assigned to C–Si (284.2 eV), CN (287 eV), CO (288.1 eV), and O–CO (289 eV). ,,,, …”