2024
DOI: 10.21203/rs.3.rs-4114254/v1
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Gram-Scale Synthesis of Heterogeneous Cu-MOFs Catalyst with Dual Functionalities for Late-stage Dicarbofunctionalization of Alkenes

Shuo Guo,
Lu Dong,
Hu Chen
et al.

Abstract: Multifunctional catalysts in organic synthesis are highly attractive, particularly in the construction of complex molecules. Here, we report the first example of heterogeneous Cu-MOFs catalyst with dual functions of photoredox and cross-coupling. IMU-108 can be synthesized on a gram scale from Cu(NO3)2·3H2O and 5-mercaptoisophthalic acid precursors by a simple reflux process. X-ray diffraction results revealed that IMU-108 is constructed from the in-situ bridged S-S bond between the zero-dimension metal-organi… Show more

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