2005
DOI: 10.1039/b414230f
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Green photochemistry: solar photooxygenations with medium concentrated sunlight

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Cited by 82 publications
(62 citation statements)
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“…The solution was concentrated to 30 mL, 1 mL of pyridine was added followed by 300 mg of the aminoalkylated polymers AAP1 (AAP2, AAP3 or PSDV-NH 2 ). The mixture was stirred overnight at 30 C, filtered, and washed with dichloromethane, tetrahydrofuran, methanol, and dichloromethane again. Non-bonding porphyrin was eliminated with these washings.…”
Section: Synthesis Of Polymeric Photosensitizers Ps1 To Ps4mentioning
confidence: 99%
“…The solution was concentrated to 30 mL, 1 mL of pyridine was added followed by 300 mg of the aminoalkylated polymers AAP1 (AAP2, AAP3 or PSDV-NH 2 ). The mixture was stirred overnight at 30 C, filtered, and washed with dichloromethane, tetrahydrofuran, methanol, and dichloromethane again. Non-bonding porphyrin was eliminated with these washings.…”
Section: Synthesis Of Polymeric Photosensitizers Ps1 To Ps4mentioning
confidence: 99%
“…[1,2] In this connection, microstructured reactors (MRs) [3] represent an interesting alternative to conventional photoreactors because the small size of the fluidic channels leads to higher spatial illumination homogeneity and better light penetration through the entire reactor depth. Also, the elevated surfaceto-volume ratio features of MRs allow an effective reagent mixing, enhanced heat-and mass-transfer rates and safer processing of toxic or highly reactive compounds.…”
Section: Introductionmentioning
confidence: 99%
“…No photoacylation reaction was detected when water, EtOH; MeOH; 1-ButOH;1-PrOH and DMK were employed as the solvent media. It is worth to note that precedents on the photoacylation of naphthoquinone 1 with butyraldehyde in t-BuOH and in 3:1 t-ButOH/DMK mixture, employing artificial 11,12 and solar light, 13 gave the respective acylhydroquinone in 84 and 90% yield, respectively. In the light of these precedents and taking into account the above results on the influence of the solvent media on the photoacylation to produce acylated hydroquinone 2, we wanted to examine the effect of binary and ternary green solvent mixtures on the photoacylation of quinone 1 with furfural.…”
Section: Experimental Generalmentioning
confidence: 99%