2008
DOI: 10.1002/sia.2944
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High oxygen vacancy tin oxide synthesized by combustion chemical vapor deposition (CCVD)

Abstract: aTin oxide nanotentacles were synthesized by combustion chemical vapor deposition in air. Their surface composition and optical properties were then investigated using X-ray photoelectron spectroscopy (XPS) and Raman spectroscopy. XPS core level spectra indicate that these nanotentacles are of high oxygen vacancy with chemical composition of about SnO 1.6 , which is also supported by the Sn Auger parameter. Besides SnO 2 , the optical properties of SnO were detected in Raman spectrum. Moreover, two new Raman p… Show more

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Cited by 25 publications
(12 citation statements)
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“…Figure 1 shows the Raman spectrum collected on the surface of a pellet obtained by hot pressing SnO 2 powder. The spectrum is charaterized by the presence of three peaks located at about 478, 633 and 776 cm −1 corresponding to the E g , A 1g and B 2g modes in good agreement with those observed in a single-crystal SnO 2 or poly-microcrystalline films 34 . Three broader and less intense bands can be observed at 350 cm −1 and between 400 and 800 cm −1 .…”
Section: Resultssupporting
confidence: 80%
“…Figure 1 shows the Raman spectrum collected on the surface of a pellet obtained by hot pressing SnO 2 powder. The spectrum is charaterized by the presence of three peaks located at about 478, 633 and 776 cm −1 corresponding to the E g , A 1g and B 2g modes in good agreement with those observed in a single-crystal SnO 2 or poly-microcrystalline films 34 . Three broader and less intense bands can be observed at 350 cm −1 and between 400 and 800 cm −1 .…”
Section: Resultssupporting
confidence: 80%
“…Figure 8 shows the Raman spectra of SnO2 nanoparticles. The spectrum is analysed by the presence of three peaks located at about 478, 633 and 776 cm -1 which are in good agreement with those observed in rutile SnO2 single crystal [16,17]. The peak at 478 cm -1 can be assigned to the Eg mode, the peak at 633cm -1 can be indexed to the A1g mode, and the peak at 776 cm -1 can be indexed to the B 2g mode.…”
Section: Figure 4 Absorption Spectrum Of Sno2 Nanoparticlessupporting
confidence: 72%
“…1B. The SnO 2 sample is characterized by a broad and structure-less band in the 450-650 cm -1 range, attributed to the presence of the amorphous SnO 2 phase [29] Moreover, a peak is barely visible at 633 cm −1 , corresponding to A 1g mode in good agreement with those observed in a single-crystal SnO 2 or poly-microcrystalline films [30]. The little shifting of D band was correlated with the structural changes, determined by the chemical bond interaction between GO and SnO 2 .…”
Section: Structural Characterizationssupporting
confidence: 65%