2019
DOI: 10.1080/10826076.2019.1645029
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High performance liquid chromatographic separation of platinum (II), gold (III), vanadium (IV), vanadium (V), molybdenum (VI) and analysis of cis-platin as platinum (II) in cis-plasol injection, urine, and blood serum using pyridoxal-4-phenyl-3-thiosemicarbazone as complexing reagent

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Cited by 3 publications
(3 citation statements)
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“…An interesting chromatogram exhibited the retention time for ligand and metal complexes Mo(VI), Ag(I), V(V), Mn(II), Pt(II), Au(III) as 2.50, 3.20, 4.80, 5.8, 6.7, 7.2, 8.5 minutes respectively. The excess amount of the derivatizing reagent that was introduced for separation eluted rst and had no impact on the determination of the metal complexes [54,55]. All complexes were separated completely after the ligand (Fig.…”
Section: Effect Of Eluents On the Retention Time Of Metal Complexesmentioning
confidence: 99%
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“…An interesting chromatogram exhibited the retention time for ligand and metal complexes Mo(VI), Ag(I), V(V), Mn(II), Pt(II), Au(III) as 2.50, 3.20, 4.80, 5.8, 6.7, 7.2, 8.5 minutes respectively. The excess amount of the derivatizing reagent that was introduced for separation eluted rst and had no impact on the determination of the metal complexes [54,55]. All complexes were separated completely after the ligand (Fig.…”
Section: Effect Of Eluents On the Retention Time Of Metal Complexesmentioning
confidence: 99%
“…HPLC methods were developed to analyze cis-platin by pre-column derivatization of Pt(II) with Schiff-base reagents pyrithione [49], n-butyl-2naphthyl dithiocarbamate [50], 2-acetylpyridine-N-phenylhydrazonecarbothioamide, N,N-bis(salicylidene)-1,2-propanediamine, bis(salicylaldehyde) tetramethyl ethylenediimine and pyridoxal-N-phenylhydrazonecarbothioamide [51][52][53][54].…”
Section: Introductionmentioning
confidence: 99%
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