2003
DOI: 10.1063/1.1593834
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High-resolution domain imaging on the nonpolar y-face of periodically poled KTiOPO4 by means of atomic force microscopy

Abstract: The inverse piezoelectric effect is used to produce high-resolution images of ferroelectric domains in periodically poled KTiOPO4 crystals on their nonpolar y-face using atomic force microscopy. We demonstrate that the technique is convenient for studying the nucleation and growth of domains in a periodically poled KTiOPO4 sample.

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Cited by 20 publications
(14 citation statements)
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“…9 The obtained pattern then is observed by optical microscopy, electron microscopy, or scanning probe microscopy techniques. 10,11 In KTP, only z-faces can be etched, 12 whereas in the common nonlinear materials LN and lithium tantalate (LT) domains on z-and y-faces can be visualized by selective etching. 13 Another standard method is Piezoresponse Force Microscopy (PFM), a derivative of atomic force microscopy, which is directly sensitive to domain walls (DWs) and domain orientation.…”
Section: Introductionmentioning
confidence: 99%
See 1 more Smart Citation
“…9 The obtained pattern then is observed by optical microscopy, electron microscopy, or scanning probe microscopy techniques. 10,11 In KTP, only z-faces can be etched, 12 whereas in the common nonlinear materials LN and lithium tantalate (LT) domains on z-and y-faces can be visualized by selective etching. 13 Another standard method is Piezoresponse Force Microscopy (PFM), a derivative of atomic force microscopy, which is directly sensitive to domain walls (DWs) and domain orientation.…”
Section: Introductionmentioning
confidence: 99%
“…11,14 However, selective etching and PFM offer only information about the surface appearance of domains, whereas this can differ from the domain structure in depth. 12 Interior views of domain structures with both methods can only be obtained with high effort and at the cost of the non-invasive character.…”
Section: Introductionmentioning
confidence: 99%
“…These findings are explained by the electric field poling process [32]. For our crystal the periodic electrode pattern was deposited on the top surface from where the domains grew in the shape of a needle towards the other electrode on the bottom side.…”
Section: Second Harmonic Generation At 423nm In Ppktpmentioning
confidence: 97%
“…(1) to the obtained set of mismatch parameters, after substituting Eqs. (7) and 4 method to five different PPKTP crystals. The tuning curve of one of these crystals is shown in Fig.…”
Section: Maker Fringes In Temperature Dependence Of Shgmentioning
confidence: 99%
“…The quality of the fabricated poling structure is generally characterized via imaging of the domain boundaries at the crystal surface. Important techniques comprise surface-charge selective etching [4], electrostatic force microscopy [5], secondary-electron microscopy [6], and piezoresponse-assisted atomic force microscopy [7]. Another way to characterize the poling quality is by studying the phase-matching conditions of a second-order nonlinear process like SHG or SPDC.…”
Section: Introductionmentioning
confidence: 99%