Due to the increase in the applications of foils, fibres, and yarns under dynamic loading, characterizing the behaviour of small-scaled material samples at high strain rates has become important. However, owing to the low mechanical impedance and the small size of such samples, the conventional split Hopkinson bar technique encounters serious problems, such as high noise-to-signal ratios, an undistinguishable transmitted signal, a short loading time, and difficulty in achieving large strain. A mini-split Hopkinson tensile bar (mini-SHTB) system has been developed to measure the constitutive relation of micro-scaled material specimens under high strain rates. The system employs polymeric bars of small diameter to achieve a closer impedance match with the specimens. This match ensures a lower noiseto-signal ratio in the transmitted signals and hence allows correct interpretation of the transmitted strain profiles. A series of experiments were carried out on different types and forms of material, such as aluminium foil, cellulose nitrate foil, badminton racket string, and so forth, to verify the applicability of the apparatus. Strain rates in the order of 10 2 were attained under this mini-SHTB system. The results confirm that the tensile stress-strain behaviour of small-sized specimens, with low mechanical impedance and under high strain rates, can be determined effectively and efficiently using this technique.