A hybrid of TiB whiskers and TiC particles reinforced TC4 matrix composites were in-situ synthesized by spark plasma sintering (SPS) using a TC4-0.6wt.% B4C powder mixture at temperatures range from 550°C to 1150°C. The effect of sintering temperature on microstructure, grain size, mechanical properties and densification process of the (TiB+TiC)/ TC4 matrix composites were investigated. The composite sintered at 1050℃ has the highest tensile strength (1129.0 MPa), yield strength (1077.8MPa) and plasticity (7.1%). The aspect ratio of TiB whiskers increases almost linearly below 1050°C and its highest value is 33.2. The grain size of TiC increases with the increase of sintering temperature, and rapid growth occurs in the range of 850°C to 950°C. The composite sintered body appears four shrinkage stages before applying sintering pressure. The corresponding peak temperatures are 663℃, 758℃, 840℃ and 994℃, respectively.