“…In addition to that, sulphide minerals (e.g., pyrite and sphalerite) Qiu and Jiang, 2007;Jiang et al, 2012), volatile-rich metamorphic minerals from hydrothermal deposits (e.g., scapolite) (Kendrick and Phillips, 2009b), and low-potassium minerals from HP/UHP metamorphic rocks (e.g., garnet) (Qiu andWijbrans, 2006, 2008) have been analyzed with some success using this dating method. In a critique of this method, Kendrick and Phillips (2009b) argued that a significant amount of lattice-hosted noble gas from scapolite can be released during prolonged crushing, but a number of studies have indicated that crushing has very little effect on the gas component that is trapped within the crystal lattice (Dunlap and Kronenberg, 2001;Qiu et al, 2002;Qiu and Jiang, 2007;Qiu and Wijbrans, 2008;Qiu et al, 2010;Jiang et al, 2012;Bai et al, 2013). This suggests that a combination of 40 Ar/ 39 Ar dating during progressive crushing and stepwise heating of the crushed powder could provide an opportunity to distinguish the gas components trapped inside fluid inclusions and on the grain boundaries of solid inclusions from the component of the gas within the crystal lattice (Villa, 2001).…”