A relationship is established between statistical characteristics of the random process of press-gradient pulsation in a fluidized bed and changes in the bed's fractional composition. This relationship can be used to monitor the process of defluidization (transition of the bed from the fluidized to the non-fluidized state) based on the results of a comparative analysis of the above-mentioned statistical characteristics. The feasibility of performing such monitoring was confirmed experimentally from the combustion of lowmelting biogranules (straw granules) in a fluidized bed. It was found that the bed remains in the fluidized state as long as the dimensionless amplitude of the pressure-gradient pulsations does not exceed 0.1. The utility of the proposed monitoring method was also substantiated by comparative studies of changes in the fractional composition of a fluidized bed and the temperature and chemical composition of the flue gases.The free movement and good mixing of particles in a fluidized bed (FB) is the most important advantage of fluidized systems. However, the particles can undergo agglomeration in certain operations carried out in FBs (drying, the application of a coating to particles, combustion and gasification of solid fuel), leading to partial or complete defluidization of the bed. Thus, it is necessary to have an effective means of diagnosing defluidization processes that will make it possible to intervene in the production process while defluidization is still early in its development and keep this phenomenon from halting the operation.Defluidization is usually identified [1, 2] by measuring temperature in the bed and in the space above it and measuring the pressure gradient inside the bed. However, such measurements are obtained too late to allow real-time intervention in the process. In addition, in some operations -such as in the combustion of straw granules in an FB -defluidization may commence 10-15 min after the beginning of the test [3]. Since defluidization is accompanied by a change in the fractional composition of the bed, it is reflected in the bed's hydrodynamics. In particular, it is reflected in the formation, ascent, and destruction of gas bubbles and associated pulsations of the pressure gradient inside the bed. Thus, the formation of agglomerates in a fluidized bed should affect the statistical characteristics of the random process of pressure-gradient pulsation in the bed [4]. However, the approaches that were used in [4][5][6] to determine these characteristics are suited only for low fluidization numbers and beds of fine particles.To study defluidization, we chose to examine the combustion of straw granules inside an FB. The characteristics of the granules are shown in Table 1.Defluidization was modeled by converting a bed from the fluidized to the non-fluidized state, i.e., we assumed that the statistical characteristics obtained when the particles comprising the bed settle are the same as in the case of fluidization.An experimental boiler plant ( Fig. 1) was used to conduct...