“…Nickel aluminides, especially NiAl, have been attracted many interests in industrial applications due to their wonderful properties such as wide composition range, high melting point, high oxidation, and hot corrosion resistance at high temperatures and low density [1][2][3][4][5]. Also, NiAl has good tribological properties [6,7]; however, sole NiAl materials contain low toughness and poor ductility at ambient temperature and poor strength and creep resistance at high temperatures which restricts its hightemperature applications [8,9]. Based on previous studies, the reduction of crystallite and particle sizes of NiAl [4,[10][11][12] and fabrication of In-situ composite [13,14] can improve the mechanical properties of NiAl.…”