Noise pollution is the cause of many health problems, and the inhabitants of the neighborhoods from crowded cities exposed to high noise is growing in Europe. Noise from thermal power plants represents the main factor of the acoustic discomfort in the residential buildings for the occupants, but also for the people who operate the equipment. The goal of this article is the experimental analysis of the efficiency of acoustic treatment solutions and their effect in reducing the noise level inside thermal power plants. Although the thermal performance and efficiency of the equipment in a boiler room have increased, the noise level produced by thermal power plants has not decreased considerably. Current measurements of the sound level in boiler plants have shown an increase in the noise level due to the fact that modern burners are noisier than old atmospheric burners, the quality of materials of the burner-boiler fixing system is poor and the volume of the boiler space becomes getting smaller. Covering the burner with a housing can reduce the noise at the source because it absorbs the noise at high frequencies. Instead, this measure is less effective in terms of low frequencies which are also the best transmitted by the structure of the building to the apartments. Regarding the chimney, the noise inside it comes from the combustion process and can be a problem in new buildings for which sound insulation or outdoor installation can be recommended. Another solution to reduce the noise level is to remove the noise source. The boiler rooms must be placed from the design stage as far as possible from the apartments, in another building, in the basement of the building or at least there should be a buffer space between the living rooms and bedrooms represented by common spaces, halls, closets, storage spaces, sheds. The results obtained by the experimental comparisons proved to be satisfactory. This article is expected to assist design engineers in improving compliance with legislation, analysis, and optimization of boiler rooms.