2000
DOI: 10.1016/s0921-4534(00)00326-9
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Influence of low temperature–low oxygen pressure post-annealing on critical current density of Bi(Pb)2223/Ag superconductors

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Cited by 17 publications
(4 citation statements)
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“…Also, the volume fraction of Bi-2201 phase decreases from 10% (S1 sample) to 6% (S88 sample). Since these secondary phases reside in the grain boundaries and act as weak links in the Bi-2223 system, 10,12) decreasing of volume fraction of these phases, promotes the intergranular critical current density and reduces the weak link network of these polycrystalline samples. Also the SEM micrographs show that by decreasing precursor powder size, grain size increases after sintering.…”
Section: Characterization Of Sintered Samplesmentioning
confidence: 99%
See 1 more Smart Citation
“…Also, the volume fraction of Bi-2201 phase decreases from 10% (S1 sample) to 6% (S88 sample). Since these secondary phases reside in the grain boundaries and act as weak links in the Bi-2223 system, 10,12) decreasing of volume fraction of these phases, promotes the intergranular critical current density and reduces the weak link network of these polycrystalline samples. Also the SEM micrographs show that by decreasing precursor powder size, grain size increases after sintering.…”
Section: Characterization Of Sintered Samplesmentioning
confidence: 99%
“…10,11) Our previous results show that the Bi-2212 phase exists within the grain boundaries and plays a role of weak links. 11) Deng et al 12) also observed, using scanning electron microscopy, that the residual Bi-2212 phase is situated at the grain boundaries of Bi-2223 phase and decreases the critical current density. Since the discovery of Bi-2223 superconductor, great progress has been achieved in enhancing the Bi-2223 phase fraction in this system.…”
Section: Introductionmentioning
confidence: 97%
“…No more than 15% of residual secondary phase Bi2212 has been detected in our compacted Bi2223 samples by x-ray diffraction studies. Note, that the residual Bi2212 phase localizes, mainly, at grain boundaries of the Bi2223 phase [18].…”
Section: Methods Of Preparation and Samplesmentioning
confidence: 99%
“…It has been believed that, in this case, the number of related phases (2212, 2201, Ca 2 PbO 4 , etc.) is reduced [3], contacts between crys tallites are improved, and the critical current increases [4,5]. According to Zhang et al [6], during annealing at a low oxygen content, particles of the Ca 2 PbO 4 phase either are not formed at all or dissolve because of the decrease in the oxidation number of Pb from 4+ to 2+, and the Pb 2+ ions are incorporated into the 2223 matrix, where they occupy the Bi positions.…”
Section: Introductionmentioning
confidence: 99%