Influence of substrate roughness on adhesion of TiN coatings

Miletić, Aleksandar; Terek, Pal; Kovačević, Lazar; Vilotić, Marko; Kakaš, Damir; Škorić, Branko; Kukuruzović, Dragan

doi:10.1007/s40430-013-0102-2

Cited by 26 publications

(10 citation statements)

References 27 publications

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“…According to the mechanical interlocking mechanism, the adhesion strength can be enhanced by increasing the interfacial bonding area, while shrinkage of the solidified BMP does not occur until the anchoring parts are pulled out. 34,35 Protein affinity…”

Section: Surface Characterizationmentioning

confidence: 99%

Enhancement of osseointegration by direct coating of rhBMP-2 on target-ion induced plasma sputtering treated SLA surface for dental application

et al. 2016

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Owing to the excellent bioactive properties of recombinant human bone morphogenetic proteins (rhBMPs), dentistry considers them as a fascinating adjuvant alternative for enhancing bone regeneration and bone-to-implant junction in the early implantation stages. However, stable loading and delivery efficiency of rhBMPs on the implant surfaces involve major concerns because of the harsh wearing condition under load during implantation. In this study, to achieve successful rhBMP-2 delivery, a nanoporous surface structure is introduced on the sandblasting with large grit and acid-etching (SLA)-treated titanium (Ti) surface via the tantalum (Ta) target-ion induced plasma sputtering (TIPS) technique. Unlike oxidation-induced surface nanoporous fabrications on a Ti surface, TIPS-treated surfaces provide excellent structural unity of the nanoporous structure with the substrate due to their etching-based fabrication mechanism. SLA/TIPS-treated Ti exhibits distinct nanoporous structures on the microscale surface geometry and better hydrophilicity compared with SLA-treated Ti. A sufficiently empty nanoporous surface structure combined with the hydrophilic property of SLA/TIPS-treated Ti facilitates the formation of a thick and uniform coating layer of rhBMP-2 on the surface without any macro- and microcoagulation. Compared with the SLA-treated Ti surface, the amount of coated rhBMP-2 increases up to 63% on the SLA/TIPS-treated Ti surface. As a result, the in vitro pre-osteoblast cell response of the SLA/TIPS-treated Ti surface, especially cell adhesion and differentiation behaviors, improves remarkably. A bone-regenerating direct comparison between the rhBMP-2-coated SLA-treated and SLA/TIPS-treated Ti is conducted on a defective dog mandible model. After 8 weeks of implantation surgery, SLA/TIPS-treated Ti with rhBMP-2 exhibits a better degree of contact area for the implanted bone, which mineralizes new bones around the implant. Quantitative results of bone-in-contact ratio and new bone volume also show significantly higher values for the SLA/TIPS-treated Ti with the rhBMP-2 specimen. These results confirm that an SLA/TIPS-treated surface is a suitable rhBMP-2 carrier for a dental implant to achieve early and strong osseointegration of Ti dental implants.

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Section: Surface Characterizationmentioning

confidence: 99%

Enhancement of osseointegration by direct coating of rhBMP-2 on target-ion induced plasma sputtering treated SLA surface for dental application

et al. 2016

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“…Some of the previous studies revealed the overestimation of hardness and Young's modulus due to the friction, while other studies reported that the friction does not affect a P-h curve significantly. For this reason, the friction between the indenter and the sample surfaces has been taken into account in some studies [6,9,18]. Additionally, it is found that the existence of friction leads to a lower amount of pileup, which is complied with the idea of Begley et al [41] that friction prevents the sliding of the material on the sides of the indenter.…”

Section: Finite Element Simulationmentioning

confidence: 86%

“…The progress toward weight reduction made possible by increasing the use of light alloys based on Al, Ti and Mg. Due to the increase in cutting temperatures and contact forces, common solutions are provided including improved superalloys based on Ni on the one hand and intermetallic materials such as TiAl and TiAlN on the other hand [1]. In this approach, the transition nitride coatings have given a great attention by the researchers for more than thirty years [6]. Among others, titaniumbased coatings are broadly used in industrial fields such as machine tools, aerospace and semiconductor technologies as well as in some medical applications [7].…”

Section: Introductionmentioning

confidence: 99%

Nanoscale characterization of Titanium-based coatings plastic properties by dimensional analysis, FEA and Infimum resultant error criterion

Bazzaz

Darvizeh

Alitavoli

et al. 2020

J Braz. Soc. Mech. Sci. Eng.

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Working with continuously harder materials and higher cutting speeds requires novel mechanical properties for cutting tools. The application of titanium-based coatings deposited by PVD is experienced as one of the most effective solutions. To assure achievement of the required characteristics in the metal cutting process, which mainly includes turning, milling, drilling and some other methods, extracting the plastic properties has been the main challenge for a long time. In this paper, a hybrid method emerging the modified dimensional analysis method (MDAM) and experimental data with novel algorithm named as minimum resultant error method is proposed. By using this algorithm, yield stress, strain hardening exponent and strain hardening coefficient are extracted as unique measures via using a single indenter nanoindentation result. An existing experimental output data and numerical solution of TiN thin film nanoindentation test are used to verify the proposed approach. The same procedure is implemented to calculate the plastic properties of TiAlN coating. Some of the results for TiAlN are among the rarely investigated matters. The effects of mesh refinement, friction coefficient and indenter tip radius are elucidated. According to the results attained from the new approach, there is an excellent agreement between MDAM and the combined algorithm results (4% for yield stress and 7% for strain hardening exponent). The resultant error is calculated in the range of 0.47-4.1% for optimized deviation. To provide another criterion of the adaptability of the results, the elastic modulus and hardness are calculated within less than 5% and 9% errors, respectively.

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“…For this purpose after coating deposition, the sandblasted process is performed. Miletica et al [48] found that the formation of the first adhesion failure (L c1 ) is hindered when a great amount of plastic deformation is needed, and the rough surfaces with asperities require more energy for getting plastically deformed. For all tested coatings, only L c2 and L c3 failures are observed.…”

Section: Discussionmentioning

confidence: 99%

The influence of plasma-sprayed coatings on surface properties and corrosion resistance of 316L stainless steel for possible implant application

Woźniak

Staszuk

Reimann

et al. 2021

Archiv.Civ.Mech.Eng

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Herein, we analyzed the morphology of atmospheric plasma-sprayed (APS) coating on medical 316L stainless steel and its influence on the physical and electrochemical properties of implant application. Five types of coatings were examined: hydroxyapatite (HAp), titanium (Ti), zirconium (Zr), Ti/HAp and Zr/HAp. The base properties of the coatings were analyzed via chemical and phase composition, surface topography, surface wettability and in particular the corrosion resistance in Ringer solution in immersed conditions and potentiodynamic test, and EIS analysis. APS coating of pure HAp on 316L stainless steel showed poor cohesive bonding to the substrate material, whereas the application of Ti and Zr interlayer prior to HAp deposition improved surface morphology and coating properties. The beneficial effect of Ti and Zr interlayer under HAp layer on binding was demonstrated. HAp containing coatings (HAp, Ti/HAp and Zr/HAp) show Ca/P ratio greater than 1.8, which may positively influence the differentiation of osteogenic cells and good adhesion to bones. Among the studied materials, the composite coatings with Zr or Zr/HAp showed favorable physicochemical properties and the highest corrosion resistance in Ringer solution.

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Influence of substrate roughness on adhesion of TiN coatings

Cited by 26 publications

References 27 publications

Enhancement of osseointegration by direct coating of rhBMP-2 on target-ion induced plasma sputtering treated SLA surface for dental application

Enhancement of osseointegration by direct coating of rhBMP-2 on target-ion induced plasma sputtering treated SLA surface for dental application

Nanoscale characterization of Titanium-based coatings plastic properties by dimensional analysis, FEA and Infimum resultant error criterion

The influence of plasma-sprayed coatings on surface properties and corrosion resistance of 316L stainless steel for possible implant application

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