Abstract:Pure b-Si 3 N 4 is used in the present work as the starting powder to synthesize a-sialon (a ) ceramics; 5 wt.% a -seeds are added to promote nucleation of a-sialon. Transmission electron microscopy (TEM) observations reveal an inhomogeneous microstructure in which intergranular precipitates are produced in some regions where the structure and the chemistry of the interfaces vary significantly. The surfaces of the sialon grains adjacent to the precipitates are always rounded and corrugated, and the interfacial… Show more
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