Infrarot-Spektroskopie diffus reflektierender Proben

Korte, Ernst‐Heiner

doi:10.1007/978-3-642-75204-9_3

Cited by 8 publications

(1 citation statement)

References 117 publications

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“…(1)), providing linear interrelation between the band intensity and the sample concentration, improved base line progression, and better resolution. 18,19 FðRÞ…”

Section: (1) Materialsmentioning

confidence: 99%

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂

Finke

Lingenfelser

Bindler

et al. 2009

Journal of the American Ceramic Society

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This paper deals with the specific interaction of the dispersant 3,6,9‐trioxadecanoic acid (TODA) with nano‐ZrO2 surfaces. Special interest was directed towards degradation behavior of the adsorbates and its influence on dispersant capabilities of TODA regarding stabilization of ethanolic nano‐ZrO2 suspensions. ZrO2 adsorption sites and the adsorbates formed are examined by diffuse reflectance infrared Fourier transform spectroscopy, thermal analysis, 1H‐, and 13C‐cross polarization magic angle spinning solid‐state nuclear magnetic resonance spectroscopy. 1H as well as 13C‐chemical shifts and the configurations of the corresponding adsorbed TODA species on zirconia sites are predicted by means of density functional theory quantum chemical calculations for supporting the interpretation of the experimental spectral data obtained. This work shows that combination of analytical and theoretical methods is an effective approach characterizing surface chemical properties of ceramic materials, determining sorption properties of organic process additives, investigating correspondent elementary and degradation reactions as well as clarifying cause‐effect relationships in ceramic processes.

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“…(1)), providing linear interrelation between the band intensity and the sample concentration, improved base line progression, and better resolution. 18,19 FðRÞ…”

Section: (1) Materialsmentioning

confidence: 99%

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂

Finke

Lingenfelser

Bindler

et al. 2009

Journal of the American Ceramic Society

View full text Add to dashboard Cite

show abstract

References

1995

Infrared and Raman Spectroscopy

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Diffuse Reflectance Infrared Fourier Transform Spectroscopy: an In situ Method for the Study of the Nature and Dynamics of Surface Intermediates

Drochner

Vogel

2012

Methods in Physical Chemistry

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Infrarot-Spektroskopie diffus reflektierender Proben

Cited by 8 publications

References 117 publications

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂

References

Diffuse Reflectance Infrared Fourier Transform Spectroscopy: an In situ Method for the Study of the Nature and Dynamics of Surface Intermediates

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Infrarot-Spektroskopie diffus reflektierender Proben

Cited by 8 publications

References 117 publications

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO2

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO2

References

Diffuse Reflectance Infrared Fourier Transform Spectroscopy: an In situ Method for the Study of the Nature and Dynamics of Surface Intermediates

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Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂

Surface Chemical Characterization of Ceramic Materials: Adsorption and Degradation of 3,6,9‐Trioxadecanoic Acid on Nano‐ZrO₂