Ultrahigh vacuum (UHV) magnetic force microscopy (MFM) was used to investigate the magnetic structure of 10 nm thick Fe films. The films were deposited on 50 nm thick Ag films on GaAs(100)/Fe substrates. The film structure was characterized in situ by scanning tunneling microscopy (STM) and low-energy electron diffraction (LEED), showing that the films grow (100)-oriented and that they display a distinct topographic texture. MFM shows that for the as-grown films the magnetization lies within the surface plane. A clear magnetic ripple structure could be identified. Rather irregular domains and 90 • domain walls were also imaged. The wall profiles are of Néel type.Thin film magnetism has attracted considerable interest over the past 50 years. This interest has recently been further boosted by the identification of the giant magnetic resistance in thin magnetic multilayers [1]. Various magnetic imaging techniques, such as the Bitter technique, Kerr microscopy or several methods based on electron microscopy, have been used to image the domain distribution of magnetic thin film samples with high resolution.Following the development of the scanning tunneling microscope (STM) [2] and the scanning force microscope (SFM) [3], the magnetic force microscope (MFM) has emerged as an additional tool for high-resolution imaging of magnetic structures of bulk and thin film samples [4]. MFM allows detection of the lateral distribution of the magnetic stray field in the near-surface region above ferromagnetic samples. On the one hand, this can be used to image the domain distribution of the sample, while on the other hand the stray field distribution also contains important information on the internal fine structure of domain boundaries. MFM imaging can therefore be used to probe the micromagnetism of thin film samples sensitively [5][6][7].Most instrumental SFM/MFM setups are operated under atmospheric conditions. In the case of MFM investigations of thin film samples this generates the problem that thin films * Corresponding author of magnetic metals, which are commonly rather reactive, either have to be protected by a passivation layer (commonly a thin noble metal layer) or that the near-surface region is oxidized and contaminated. As a result the crucial near-surface region will be structurally and electronically altered, leading to possible ambiguities in the correlation of MFM images to the micromagnetic structure.The influence of surface contamination can be greatly reduced by performing the deposition and the MFM characterization of thin film samples in situ in UHV. Here, the first results of a comprehensive UHV MFM study on thin Fe films are presented, where the samples are grown in UHV. They were first characterized by Auger electron spectroscopy (AES), low-energy electron diffraction (LEED) and STM before probing the magnetic structure by MFM.
ExperimentalFor the study a UHV system was used in which several metal evaporators, a combined AES/LEED system, a combined secondary electron microscope (SEM)/STM system, and an S...