2020
DOI: 10.3390/separations7030039
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Investigating the Utility of Fabric Phase Sorptive Extraction and HPLC-UV-Vis/DAD to Determine Antidepressant Drugs in Environmental Aqueous Samples

Abstract: Depression is considered to be one of the most prevalent mental disorders in humans. Antidepressant drugs are released in large concentrations and cause adverse effects on the environment and/or human health. Fabric Phase Sorptive Extraction (FPSE), a contemporary solid sorbent-handling technique, is a quick, sensitive, and simple analytical process. This paper describes a micro-extraction FPSE procedure coupled with High-Performance Liquid-Chromatography–Photodiode Array Detection (FPSE-HPLC–DAD) for … Show more

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Cited by 19 publications
(12 citation statements)
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“…IR spectra were recorded on a Perkin-Elmer Spectrum One FT-IR spectrometer (Thermo Fisher Scientific, Leicestershire, UK). The mass spectra were measured with a Micromass Quattro LC/ULTIMA LC-MS/MS (Brucker Daltonik GmbH, Hamburg, Germany) spectrometer using chloroform-methanol as the solvent system for phthalonitrile (3) and with a MALDI-TOF MS (Brucker Microflex LT, Bremen, Germany) spectrometer in dihydroxybenzoic acid as MALDI matrix using nitrogen laser accumulating 50 laser shots for copper phthalocyanine (4). Melting points were measured by a Thermo Scientific 00590Q Fisher-Johns melting point apparatus, 220 VAC (Cole-Palmer, Brescia Cernusco Sul Naviglio, Milano, Italy).…”
Section: Instrumentation and Methodsmentioning
confidence: 99%
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“…IR spectra were recorded on a Perkin-Elmer Spectrum One FT-IR spectrometer (Thermo Fisher Scientific, Leicestershire, UK). The mass spectra were measured with a Micromass Quattro LC/ULTIMA LC-MS/MS (Brucker Daltonik GmbH, Hamburg, Germany) spectrometer using chloroform-methanol as the solvent system for phthalonitrile (3) and with a MALDI-TOF MS (Brucker Microflex LT, Bremen, Germany) spectrometer in dihydroxybenzoic acid as MALDI matrix using nitrogen laser accumulating 50 laser shots for copper phthalocyanine (4). Melting points were measured by a Thermo Scientific 00590Q Fisher-Johns melting point apparatus, 220 VAC (Cole-Palmer, Brescia Cernusco Sul Naviglio, Milano, Italy).…”
Section: Instrumentation and Methodsmentioning
confidence: 99%
“…These compounds have been reported to breakdown slowly or to be persistent for a longer period and/or bioaccumulate [2,3]. A wide spectrum of these compounds is found with respect to their applications ranging from pesticides to pharmaceuticals and personal healthcare products (PPCPs), to organic solvents, to endocrine disrupting compounds (EDCs), to flame retardants, to artificial sweeteners, and other industrial chemical products [1][2][3][4]. Among these compounds, is a class of pollutants referred to as contaminants of emerging concerns (CECs), anthropogenically synthesized organic chemical pollutants detected in natural water bodies at very low concentration levels [2][3][4].…”
Section: Introductionmentioning
confidence: 99%
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“…The primary material that was used for the extraction of target analytes was a Whatman microfiber glass filter (FG) coated with short-chain poly (ethylene glycol) (PEG) by sol-gel process. Details about the sol-gel coating technique, the synthesis and characterization of the FPSE media are described in previous publication of our research group [53]. Based on the aforementioned publication with some modifications the procedure was applied for the extraction of 21 analytes.…”
Section: Fabric Phase Sorptive Extraction (Fpse)mentioning
confidence: 99%
“…FPSE has been applied to extract a wide range of analytes from different samples, such as UV stabilizers in sewage samples [48], anti-inflammatory drugs [49], alkyl phenols in aqueous and soil samples [50], triazine herbicides [35], estrogens in urine and environmental water samples [51], and polar antibiotic in raw milk [52]. Our research group has recently used FPSE for the extraction of selected antipsychotic drugs from environmental waters followed by high performance liquid chromatography-UV-DAD with satisfactory results [53].…”
Section: Introductionmentioning
confidence: 99%