Due to their effectiveness, lightweight materials have gained international attention in recent decades, with industrial sectors being the primary users of them. Metal matrix composites with nanohybrid reinforcement are a unique composite system combination that enhances the material’s mechanical qualities. In the present article, the mechanical properties of graphene nanoplatelets (GNP) and titanium dioxide (TiO2)-reinforced aluminium 7075 alloy are discussed with varying weight percentages of reinforcements prepared by the stir casting technique. 1 wt.% GNP with and 3 wt.% TiO2-reinforced composites show optimum properties within the range of reinforcement studied, with a 71.9% increment in tensile strength and an 86.6% improvement in microhardness observed; however, elongation is decreased by 31.7% in contrast to the base alloy. Maximum toughness is found to be in 0.5 wt.% GNP with 1 wt.% TiO2-reinforced nanohybrid composites. XRD results show phase analysis. SEM analysis of the fractured surface reveals a mixture of ductile and brittle fractures.