“…The XRD spectrum of the Fe 1 O x sample shows diffraction peaks at 18.27°, 30.09°, 35.42°, 37.05°, 43.05°, 53.39°, 56.64°, 62.51°, and 73.94°, with the peak at 35.42° corresponding to the (311) crystal plane of Fe 3 O 4 (PDF#19‐0629), [32] which was identified as the predominant structure in the sample. In addition to peaks related to Fe 3 O 4 , the spectrum of the Ni 1 Fe 1 O x sample exhibits peaks at 44.27°, 51.53°, and 75.86°, corresponding to the (111), (200), and (220) crystal planes, respectively, of a Ni/Fe alloy (PDF#38‐0419) [33] . The peak at 43.05°, associated with Fe 3 O 4 (400), is slightly more intense in the spectrum of Ni 1 Fe 1 O x than in that of Fe 1 O x , indicating an stronger interaction between Fe and Ni; this, in addition to an increase in the diffraction intensity, may result in interference between nearby peaks.…”