Iodometric microdetermination of phosphorus, sulfur and chlorine in organic compounds

Organic elemental analysis

“…Habashy, Gawargious, and Faltaoos (110) determined the liberated halides by a polarographic tehnique. Prokopov (204) decomposed chlorine-containing samples in a closed flask and then caused iodine to be liberated which was titrated with sodium thiosulfate solution. For iodine-containing compounds, Pitre and Grand!…”