ISATOIC ANHYDRIDE. I. REACTIONS WITH PRIMARY AND SECONDARY AMINES AND WITH SOME AMIDES¹

Synthesis and Spectral Characterization of Sulfhydryl-Reactive Fluorescent Probes

“…NMIA was reacted neat in ence position. All samples were filtered through a 0.45-ethylenediamine at 35ЊC to form Intermediate 1 with mm Millipore filter to minimize light scattering and the subsequent loss of carbon dioxide gas (24). The priwere excited at 326 nm (except where noted).…”

Synthesis and Spectral Studies of Some Transition metal Complexes

“…Further amide II absorption [ν(C-H) + δ(N-H)] around 1500 cm -1 in the ligand spectrum is shifted by 55cm -1 . These shifts are of considerable magnitude and confirm that this ligand coordinates through amine and amide nitrogen atom [24][25][26][27] .…”

Novel Four-Step Synthesis of Thioxo-quinazolino[3,4-a]quinazolinone Derivatives

“…[12,15] Clearly the reaction is conducted by the nucleophilic attack of amine on the isatoic anhydride with liberation of CO 2 . [16] The second step of our synthetic scheme was preparing the 2,3-dihydro-2-(2-nitrophenyl)-3-arylquinazolin-4(1H)-one derivatives 4. A literature survey shows that there are various procedures for the one-pot, three-component synthesis of quinazolin-4(1H)-ones starting from isatoic anhydride, amines, and aldehydes.…”