“…Generally, mechanical alloying is developed from a starting mixture of pure powders, which progressively become alloyed to form an amorphous and/or a supersaturated solid solution. The study of microstructural evolution is frequently followed by X-ray diffraction (XRD) [3,4,5,6,7,8,9], characterizing the phase evolution, average values of microstructural parameters (grain size and microstrains) and compositional information derived from evolution of the average lattice parameter.…”