The stage of drying pastilles (marshmallow) is the most time-consuming and energy-consuming. Its course depends on temperature, air convection, quality of raw materials and other factors. The dynamics of moisture removal can be monitored using thermal analysis methods. These methods provide information on the kinetics of dehydration, thermal stability of components, thermal effects of moisture removal. The results of the study of semi-finished products from apples and pumpkin were obtained on a Netzsch STA 449F3 device. The obtained data can be used in the modeling of technological production processes and can reduce the time and resources spent.