This research paper reports the results for convective heat transfer coefficient and nucleate boiling heat flux for pool boiling of milk during khoa making. Various indoor experiments were conducted for different heat flux inputs varying from 9638.55 to 14457.83 W/m 2 . Experimental data obtained for pool boiling of milk were analyzed by using the Rohsenow correlation with the help of simple linear regression analysis. The convective heat transfer coefficients were estimated in the range of 334.48 to 837.78 W/m 2 °C for the given heat inputs. The results for heat flux were found to be varying from 3344.8 to 8377.8 W/m 2 at 10 °C excess temperature of the aluminum pot surface above the saturation temperature of the milk. The experimental errors in terms of percent uncertainty were also calculated.