2017
DOI: 10.1177/0263617417704310
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Lanthanide metal–organic frameworks: Structural, thermal and sorption properties

Abstract: Two coordination polymers of erbium(III) and neodymium(III) ions with 1,3,5-benzenetricarboxylic acid were synthesized under the solvothermal conditions from the dimethylformamide solution. They were characterized by the attenuated total reflectance Fourier transform spectroscopy (ATR-FTIR), thermogravimetry and differential scanning calorimetry (TG-DSC), thermogravimetric analysis coupled with Fourier transform infrared spectroscopy (TG-FTIR) and X-ray diffractions methods. The single-crystal X-ray analysis c… Show more

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Cited by 6 publications
(3 citation statements)
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“…This publication is continuation of our long-term research on coordination polymers of lanthanides with polycarboxylic acids [37,38,[47][48][49][50][56][57][58][59][60][61][62][63][64]. Herein, the influence of different synthetic approaches on structural and thermal properties of the coordination polymers based on the selected lanthanide(III) ions such as: Nd(III), Eu(III), Tb(III) and Er(III) as well as 1H-pyrazole-3,5-dicarboxylic acid (H 3 pdca) is studied.…”
Section: Introductionmentioning
confidence: 92%
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“…This publication is continuation of our long-term research on coordination polymers of lanthanides with polycarboxylic acids [37,38,[47][48][49][50][56][57][58][59][60][61][62][63][64]. Herein, the influence of different synthetic approaches on structural and thermal properties of the coordination polymers based on the selected lanthanide(III) ions such as: Nd(III), Eu(III), Tb(III) and Er(III) as well as 1H-pyrazole-3,5-dicarboxylic acid (H 3 pdca) is studied.…”
Section: Introductionmentioning
confidence: 92%
“…A Teflon-lined vessel is placed in a steel autoclave, in which the reagents are heated in high-boiling polar solvents, such as DMF, DEF, DMSO, H 2 O, acetone, acetonitrile etc. The advantage of this method is that it ensures high solubility of the precursors and the formation of good quality MOF crystals suitable for structural investigations [46][47][48][49]. Among the nonsolvothermal methods of MOF synthesis, classical precipitation and mechanochemistry can be distinguished.…”
Section: Introductionmentioning
confidence: 99%
“…Hence, the main aim of the present work was to synthesize new coordination polymers derived from p-XBTA by exploring different hydrothermal and reverse precipitation methods in aqueous medium. These methods could allow to cope with sparingly soluble ligands in water and to obtain pure crystalline products [10,11,12]. This study thus reports on the preparation, complete characterization, crystal structures, spectroscopic features, topological classification, and thermal behavior of two new polymeric 3D metal-organic architectures driven by flexible p-XBT 2− linkers.…”
Section: Introductionmentioning
confidence: 99%