Suspended particulate matter was collected every sixth day at five stations in the New York metropolitan area for one year using high-volume samplers and Whatman no. 41 filters. These samples were analyzed by emission spectrography for calcium, lead, iron, copper, aluminum, silicon, nickel, vanadium, sodium, and magnesium. This sampling and analysis procedure has the advantage of eliminating the acid extraction step common to methods in which glass-fiber collection media are employed, and of permitting Si, Al, and other elements present in glass to be determined without high blank corrections. In general, trends in the concentrations of the elements are not obvious, though most of the elements seem to follow approximately the same pattern over the year.As part of a continuing program of environmental .-studies, ambient particulate matter samples were collected, using high-volume samplers, at five sites in the New