2017
DOI: 10.1002/jccs.201600847
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Linking Bridged Tetracopper Complexes with Neutral Dipyridyl Compounds to Coordination Polymers and Discrete Metalacages

Abstract: The bridged tetracopper(I) complex [{Cu2(μ‐dppm)2}2(μ‐(1,3‐O2CC6H4 (CO2 )2)](BF4 )2 (2(BF4 )2) was prepared. This complex and the neutral dipyridyl compounds (NN; NN = 4,4′‐bipyridine (bpy), 1,2‐bis(4‐pyridyl)ethane (bpa), 4,4′‐trimethylenedipyridine (tmp)) can form dynamic equilibria in CH2Cl2 . From the equilibrium mixtures containing 2(BF4 )2 and NN with 2(BF4 )2/NN = 1:1, different supramolecular compounds were obtained as single crystals, and their structure were determined by X‐ray crystallography. The f… Show more

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