Liquid Chromatographic Resolution of Racemic 2‐Oxazolidinones and their Analogs on Seven Pirkle‐Type Chiral Stationary Phases

A C3 symmetric (R)-phenylglycinol N-1,3,5-benzenetricarboxylic acid-derived chiral stationary phase (CSP) and three C2 symmetric (R)-phenylglycinol CSPs were newly synthesized using o-, m-, and p-phthaloyl dichlorides. These CSPs were used to compare the resolution of 25 chiral samples using a previously reported 3,5-dinitrobenzoyl (R)-phenylglycinol-derived CSP. Even though all CSPs have the same chiral moiety, the C3 symmetric CSP showed the best resolution.

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Synthesis and Application of C2 and C3 Symmetric (R)‐Phenylglycinol‐Derived Chiral Stationary Phases

Ryoo

Lee

et al. 2016

Chirality

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Liquid Chromatographic Resolution of Racemic 2‐Oxazolidinones and their Analogs on Seven Pirkle‐Type Chiral Stationary Phases

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References 24 publications

Synthesis and Application of C2 and C3 Symmetric (R)‐Phenylglycinol‐Derived Chiral Stationary Phases

Synthesis and Application of C2 and C3 Symmetric (R)‐Phenylglycinol‐Derived Chiral Stationary Phases

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