2018
DOI: 10.1039/c8ce00632f
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Liquid phase deposition of iron phosphate thin films

Abstract: Liquid phase deposition (LPD) has been applied for the synthesis of iron phosphate thin films as an example of an effective methodology for the thin film growth of other polyanionic compounds.

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Cited by 7 publications
(5 citation statements)
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“…For the 0.04 M solution, 0.34 g NH 4 PF 6 , 0.82 g Fe(NO 3 ) 3 ·9H 2 O, and 0.37 g H 3 BO 3 , and for 0.08 M solution, 0.68 g NH 4 PF 6 , 1.64 g Fe(NO 3 ) 3 ·9H 2 O and 0.74 g H 3 BO 3 were dissolved in 50 mL of deionized water. 41 The back-side and the conductive part of the hematite samples were covered with scotch tape so that the hematite films were only exposed to the treatment solution. The 0.04 and 0.08 M treatment solutions were heated to 60 and 75 °C, respectively.…”
Section: Methodsmentioning
confidence: 99%
See 1 more Smart Citation
“…For the 0.04 M solution, 0.34 g NH 4 PF 6 , 0.82 g Fe(NO 3 ) 3 ·9H 2 O, and 0.37 g H 3 BO 3 , and for 0.08 M solution, 0.68 g NH 4 PF 6 , 1.64 g Fe(NO 3 ) 3 ·9H 2 O and 0.74 g H 3 BO 3 were dissolved in 50 mL of deionized water. 41 The back-side and the conductive part of the hematite samples were covered with scotch tape so that the hematite films were only exposed to the treatment solution. The 0.04 and 0.08 M treatment solutions were heated to 60 and 75 °C, respectively.…”
Section: Methodsmentioning
confidence: 99%
“…Note that the obtained data are consistent with our earlier report on the LPD of iron phosphate. 41 Raman spectroscopy was performed to study the lattice dynamics and the associated chemical bonds. Fig.…”
Section: Pec Characterizationmentioning
confidence: 99%
“…29 Thus, these materials can be obtained in many form factors such as bulk ceramics, thin films, or membrane materials. [30][31][32] Due to the different condensation degrees of the phosphate units and variable exchangeable metal cations, TMPs provide a wide range of chemical compositions.…”
Section: Introductionmentioning
confidence: 99%
“…As a result, the hydrolysis reaction () proceeds toward the formation of Fe(OH) 3 52 . Also, the thickness of the thin film can be controlled by deposition time 56 . The Fe(OH) 3 films under heat‐treatment at proper temperatures convert to hematite: FeF63badbreak+3H2normalOFeOH3goodbreak+3H+goodbreak+6F\begin{equation} {\left[\mathrm{Fe}{\mathrm{F}}_{6}\right]}^{3-}+3{\mathrm{H}}_{2}\mathrm{O}\leftrightarrows \text{Fe}{\left(\mathrm{OH}\right)}_{3}+3{\mathrm{H}}^{+}+6{\mathrm{F}}^{-} \end{equation} H3BO3badbreak+4HFBF4goodbreak+2H2normalOgoodbreak+H3O+\begin{equation} {\mathrm{H}}_{3}{\mathrm{BO}}_{3}+4\mathrm{HF}\leftrightarrows {\text{BF}}_{4}^{-}+2{\mathrm{H}}_{2}\mathrm{O}+{\mathrm{H}}_{3}{\mathrm{O}}^{+} \end{equation}…”
Section: Introductionmentioning
confidence: 99%
“…52 Also, the thickness of the thin film can be controlled by deposition time. 56 The Fe(OH) 3 films under heat-treatment at proper temperatures convert to hematite:…”
Section: Introductionmentioning
confidence: 99%