“…Nevertheless, in developing countries there is no restriction on the use of these substances. Therefore monitoring of environment pollution by pesticides is still concern in both developed and developing countries ( Analytical task: Development of low cost and sensitive methods for the determination of pesticides in the environment is needed (Andrade-Eiroa et al, 2002;Heinisch et al, 2005;Heinisch et al, 2004;Taylor & Grate, 1995;Wegner et al, 2005). For direct detection of these molecules hyphenated techniques such gas or liquid chromatography with mass spectrometry (Alder et al, 2006;Hercegova et al, 2007;Hernandez et al, 2005;Lacorte & Barcelo, 1996;Lambropoulou & Albanis, 2007;Popp et al, 1997;Rodriguez-Mozaz et al, 2007;Sancho et al, 2006), capillary electrophoresis (Boyce, 2007;Ravelo-Perez et al, 2006), thin layer chromatography (Sherma, 2007) coupled with various detectors are used.…”