Spinel CoZnTiO 4 ceramics were synthesized by conventional solid-state method and their microwave dielectric properties were investigated. The crystal structure and microstructures of specimens were studied by XRD and SEM. The CoZnTiO 4 phase forms at a temperatures ranging from 1140 to 1220°C and the dependence of the dielectric properties of the ceramics on the sintering condition is found to be insignificant. The relative densities of the specimens are higher than 95 % for the entire temperature range tested during the experiment. Specimen using CoZnTiO 4 sintered at 1200°C possesses a combination of dielectric properties with e r * 17.31, Q 9 f * 97,571 GHz (where f = 8.84 GHz, is the resonant frequency) and s f * -36.4 ppm/°C, which makes it a suitable candidate material for microwave devices.