Low‐Temperature Sn<sup>0</sup> Nanoparticles Synthesis by Means of Tin(II) N,N‐Complexes Reduction

Srb, Michael; Milasheuskaya, Yaraslava; Jambor, Roman; Kopecká, Kateřina; Knotek, Petr

doi:10.1002/slct.202100618

ChemistrySelect

2021

DOI: 10.1002/slct.202100618

|View full text |Cite

Low‐Temperature Sn⁰ Nanoparticles Synthesis by Means of Tin(II) N,N‐Complexes Reduction

Michael Srb

Yaraslava Milasheuskaya

Roman Jambor

et al.

Abstract: A novel low‐temperature liquid phase synthesis of the Sn0 nanoparticles has been reported. The effect of different reducing agents (Li[AlH4], K[BEt3H], Na[BH4]) on the reduction of the two different N,N‐coordinated SnII complexes has been described. The influence of the different imino‐pyridine chelating ligands to the synthesis of the Sn0 particles, their separation and the usage of surfactant for resuspendation to nanocolloid has been studied. The Sn0 nanoparticles were studied by means of Energy‐dispersive … Show more

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2021

2024

Publication Types

Select...

Article2

Relationship

Self Cite0

Independent2

Authors

Journals

Cited by 2 publications

References 45 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

Low‐Temperature Synthesis of GeTe Nanoparticles

Bouška,

Milasheuskaya,

Šlouf

et al. 2024

Chemistry A European J

View full text Add to dashboard Cite

Nanoparticles can offer an alternative approach to fabricate phase‐change materials. The chemical synthesis of GeTe nanoparticles using organometallic precursors exploits high‐boiling solvents and relatively high temperatures (close or even above crystallization temperatures), as reported in the available literature. The aim of this work is the preparation of GeTe nanoparticles by a low‐temperature synthetic method exploiting new organometallic precursors and common organic solvents. Indeed, different preparation methods and characterization of GeTe nanoparticles is discussed. The characterization of the prepared nanomaterial was performed on the basis of X‐ray diffraction, transmission electron microscopy, scanning electron microscopy with energy dispersive X‐ray spectroscopy, laser ablation time‐of‐flight mass spectrometry, Raman scattering spectroscopy, and dynamic light scattering. The results show that the low‐temperature synthetic route leads to amorphous GeTe nanoparticles. Exploited organometallic precursor is stabilised by neutral ligand which can be isolated after the reaction and repeatedly used for further reactions. Furthermore, GeTe nanoparticle size can be tuned by the conditions of the synthesis.

show abstract

Low‐Temperature Synthesis of GeTe Nanoparticles

Bouška,

Milasheuskaya,

Šlouf

et al. 2024

Chemistry A European J

View full text Add to dashboard Cite

show abstract

TiO2 Modified Geopolymers for the Photocatalytic Dye Decomposition

et al. 2021

View full text Add to dashboard Cite

This article studies the photocatalytic activity of three types of industrially produced TiO2 powder (P25, CG100 and CG300) incorporated into a parent geopolymer matrix, and their pure counterparts, based on the decomposition of Rhodamine B dye. Rhodamine B dye is applied as a model substance because it is frequently used in the textile industry and thus may be present in the wastewater. The average particle size, specific surface area and mineralogical composition of TiO2 powders have been determined. The geopolymer matrix works well as a supporting material for the CG100 and P25 pure types of TiO2 powder as these input materials have better properties such as a higher average particle size, lower specific surface area, mineralogicalcomposition, etc., than the CG300 TiO2 powder. These properties (or their combination) affect the photocatalytic activity of the resulting materials, which may thus become advanced composites with an additional purifying ability, e.g., materials that can be used for wastewater treatment or air purification.

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

This site is protected by reCAPTCHA and the Google Privacy Policy and Terms of Service apply.

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

Low‐Temperature Sn⁰ Nanoparticles Synthesis by Means of Tin(II) N,N‐Complexes Reduction

Cited by 2 publications

References 45 publications

Low‐Temperature Synthesis of GeTe Nanoparticles

Low‐Temperature Synthesis of GeTe Nanoparticles

TiO2 Modified Geopolymers for the Photocatalytic Dye Decomposition

Contact Info

Product

Resources

About

Low‐Temperature Sn0 Nanoparticles Synthesis by Means of Tin(II) N,N‐Complexes Reduction

Cited by 2 publications

References 45 publications

Low‐Temperature Synthesis of GeTe Nanoparticles

Low‐Temperature Synthesis of GeTe Nanoparticles

TiO2 Modified Geopolymers for the Photocatalytic Dye Decomposition

Contact Info

Product

Resources

About

Low‐Temperature Sn⁰ Nanoparticles Synthesis by Means of Tin(II) N,N‐Complexes Reduction