2010
DOI: 10.4314/bcse.v24i1.52964
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<b>Preparation of diethyl malonate adducts from chalcone analogs containing a thienyl ring</b>

Abstract: Nine chalcone-diethyl malonate derivatives (4a-i) were prepared by the reaction of chalcone derivatives (3a-i) with diethyl malonate in the presence of a catalytic amount of KOt-Bu in CH2CI2 in good to excellent yields. The products were characterized by FTIR, 1 H-NMR, 13 C-NMR and elemental analyses.

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Cited by 4 publications
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“…A doublet at 7.55 ppm corresponds to 4 and 5 th position protons of thiophene ring. These peaks confirm the formation of the compounds [10,11]. The compound formation was confirmed by the recorded H 1 NMR spectra and they reveal the substitution to 2-position of thienyl ring in 2-CTP causing a downfield shift of approximately 0.9 -1 ppm from the substitution to 3-position of thienyl ring in 3-CTP.…”
Section: Growth Of 2-ctp and 3-ctp Single Crystalssupporting
confidence: 66%
“…A doublet at 7.55 ppm corresponds to 4 and 5 th position protons of thiophene ring. These peaks confirm the formation of the compounds [10,11]. The compound formation was confirmed by the recorded H 1 NMR spectra and they reveal the substitution to 2-position of thienyl ring in 2-CTP causing a downfield shift of approximately 0.9 -1 ppm from the substitution to 3-position of thienyl ring in 3-CTP.…”
Section: Growth Of 2-ctp and 3-ctp Single Crystalssupporting
confidence: 66%