LXIV.—Syntheses by means of magnesium amyl halides

Davies, W. Cule; Dixon, R. S.; Jones, Walter W.

doi:10.1039/jr9300000468

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Experimental112

Synthesis and Purification Of The Hydrocarbons1

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1933

1963

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Cited by 16 publications

(3 citation statements)

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“…The crude products from four Grignard reactions (9 moles of benzaldehyde) were combined and distilled under reduced pressure in the glass-helix packed column. The fractions boiling at 172 °C at 50 mm Hg, normalnnormalD20 1.5064 to 1.5048 [13], were collected as 1-phenyl-1-hexanol. The yield was 1264 g (7.1 moles) which represents 79 percent yield on the basis of benzaldehyde used; a total of 4.5 kg was prepared.…”

Section: Synthesis and Purification Of The Hydrocarbonsmentioning

confidence: 99%

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Mears¹,

Stanley²,

Compere³

et al. 1963

J. RES. NATL. BUR. STAN. SECT. A.

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As par t of a program to det ermine acc urat ely t he heat s of combustion of speciali zed fuels in the kerose ne range, seve n hydrocarbons, biphenyl, bicyclohexyl, cyclohexylbenze lle, n-hexylbe nzene, n-hexylcyclohexa ne, l -cyclope nty lheptane, a nd n-dodecane were sy nthesize d or purified from co mmercial mate ri a l. Physical co nstants were det ermined on the purified samples. These materials may have use as seco ndary stan da rds for heat of co mbu stion meas urem ents.

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Section: Synthesis and Purification Of The Hydrocarbonsmentioning

confidence: 99%

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Mears¹,

Stanley²,

Compere³

et al. 1963

J. RES. NATL. BUR. STAN. SECT. A.

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“…These reactions (Exps. [20][21][22][23] were carried out essentially as described for Exp. 11, and the products were worked up as described for Exp.…”

Section: Experimental11mentioning

confidence: 99%

Influence of the Metallic Cation of Certain Organometallic Compounds on the Courses of Some Organic Reactions^1,2

O'Sullivan¹,

Swamer²,

Humphlett³

et al. 1961

J. Org. Chem.

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“…acad. Lincei, [5] 13, I, 39 (1904); Benary, Ber,, 44, 493 (1911); Gilman, Burtner and Smith, Rec. trav.…”

Section: Experimental Partmentioning

confidence: 99%

Orientation in the Furan Nucleus. III. 5-Methyl-3-furoic Acid¹

Gilman¹,

Burtner²,

Smith³

1933

J. Am. Chem. Soc.

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LXIV.—Syntheses by means of magnesium amyl halides

Cited by 16 publications

References 0 publications

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Influence of the Metallic Cation of Certain Organometallic Compounds on the Courses of Some Organic Reactions^1,2

Orientation in the Furan Nucleus. III. 5-Methyl-3-furoic Acid¹

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LXIV.—Syntheses by means of magnesium amyl halides

Cited by 16 publications

References 0 publications

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Synthesis, purification, and physical properties of seven twelve-carbon hydrocarbons

Influence of the Metallic Cation of Certain Organometallic Compounds on the Courses of Some Organic Reactions1,2

Orientation in the Furan Nucleus. III. 5-Methyl-3-furoic Acid1

Contact Info

Product

Resources

About

Influence of the Metallic Cation of Certain Organometallic Compounds on the Courses of Some Organic Reactions^1,2

Orientation in the Furan Nucleus. III. 5-Methyl-3-furoic Acid¹