“…Recently, transition-metal oxide (TMO) nanomaterials have displayed various attractive, dimensional, and morphological properties for diverse applications in research fields such as chemistry, materials science, physics, and biology. − Recently, Fardood et al have investigated various mixed TMOs for a large number of dye-degradation reactions under ambient conditions. ,,,, Among the TMOs, Co 3 O 4 has played a promising role as a p-type semiconducting material which is widely used as photocatalyst or photoanode material for electrochemical and solar energy applications. − The magnetic properties of Co 3 O 4 nanomaterials might originate because of spin–orbit coupling of unpaired electrons in partially filled orbitals of Co 2+ cations. Owing to fully filled t 2g 6 orbitals, Co 3+ cations display zero magnetic moment after the 3d splitting by the low-spin octahedral crystal field. , Among binary metal-oxide nanomaterials, nickel–cobalt oxides are well-known p -type semiconducting nanomaterials which have an energy band gap in the range of ∼1.48 to ∼2.30 eV to tune their electronic, optical, surface morphological, and magnetic properties. − Moreover, nickel–cobalt oxides are cost-effective, naturally abundant, less toxic materials with a variety of morphologies and high redox properties resulting in wide range of optical and electronic applications. − In general, cobalt based nanomaterial possesses versatile fascinating properties including low toxicity, magnetic nature, high stability, and excellent chemical reactivity because of variable oxidation states, for example, a spinel crystal geometry which are suitable for electrochromic, sensor, and catalytic applications. − Furthermore, binary nickel–cobalt oxide (NiCo 2 O 4 , NCO) nanomaterials exhibit a spinel crystal structure where Ni cations reside in octahedral positions only, while Co cations spread on octahedral and tetrahedral positions of the crystal lattice, simultaneously. , NiCo 2 O 4 inherits many intriguing properties such as eco-friendly synthesis, a porous surface morphology, high surface area, and excellent stability to ensure high performance as an electrode material . Recently, NiCo 2 O 4 has been reported to possess distinct morphologies such as nanorods, nanowires, and nanosheets, which are tuned by their synthetic approaches. , …”