2015
DOI: 10.1002/jssc.201500519
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Magnetic octadecyl‐based matrix solid‐phase dispersion coupled with gas chromatography with mass spectrometry in a proof‐of‐concept determination of multi‐class pesticide residues in carrots

Abstract: A novel procedure is put forward based on the combination of the well-established matrix solid-phase dispersion and the magnetic and sorption properties of magnetic octadecyl in the presence of n-octanol and was employed in a proof-of-concept sample preparation and determination of several classes of pesticide residues in carrots. The procedure does not require the transfer of blend to cartridge and subsequent packing, nor any co-sorbent for extract clean up. The hydrophobic magnetic nanoparticles utilized as … Show more

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Cited by 10 publications
(4 citation statements)
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“…The content of THF in the bulk solution influences SUPRASs composition and structure and, consequently, it could affect extraction efficiency [25]. SUPRASs were prepared from a constant concentration of 1-decanol (2.4%, v/v) and varying percentages of THF (10,15,20, and 25%, v/v). Here, the total volume of the bulk solution, which the extraction device was able to take up, was considered to be 5 mL.…”
Section: Selection Of Supras-me Conditionsmentioning
confidence: 99%
See 1 more Smart Citation
“…The content of THF in the bulk solution influences SUPRASs composition and structure and, consequently, it could affect extraction efficiency [25]. SUPRASs were prepared from a constant concentration of 1-decanol (2.4%, v/v) and varying percentages of THF (10,15,20, and 25%, v/v). Here, the total volume of the bulk solution, which the extraction device was able to take up, was considered to be 5 mL.…”
Section: Selection Of Supras-me Conditionsmentioning
confidence: 99%
“…Low consumption of sample and solvents, simplicity, and the capability to simultaneously perform disruption, extraction, and clean up in a single step are some of its major advantages. MSPD has been successfully applied to the extraction of a wide variety of analytes from animal tissues, foodstuff, serum, milk, vegetables, fruits, plant materials, and other solid samples .…”
Section: Introductionmentioning
confidence: 99%
“…Apart from high selectivity, rapid solid-liquid phase separation is also desired for adsorption. Magnetic separation by an appropriate magnetic field provides a convenient and low-cost way for separation without using tedious filtration or centrifugation [22][23][24][25]. Usually, Fe 3 O 4 was used to endow materials with magnetism.…”
Section: Introductionmentioning
confidence: 99%
“…So, it is necessary to carry out efficient pretreatment before qualitative and quantitative analysis. Magnetic solid‐phase extraction (MSPE) has attracted wide attention recently as the treatment procedure is simple, efficient, rapid , economical, and ecofriendly . Due to the use of magnetic materials, the extraction procedure is dramatically simplified and extraction selectivity can be greatly improved .…”
Section: Introductionmentioning
confidence: 99%