“…The hyperfine magnetic field distributions obtained by deconvoluting the Mössbauer spectra have a width which increases with milling time, revealing that the disorder degree of the alloy increases with milling time [16,18,19]. A complete conversion to a random fcc FeeNi alloy after 3 h of milling was evidenced [16]. Also, it was found that the inoculation of nanocrystalline Ni 3 Fe germs to the NieFe mixture improves the synthesis of the Ni 3 Fe phase by combined mechanical alloying and annealing technique [23].…”