) radicals were the main reactive species for dye degradation in the present sonocatalytic system. A proposed mechanism for the enhanced photocatalytic activity is also discussed based on the experimental results. In addition, the catalytic activity of the nanocomposite in the reduction of nitrophenols by using NaBH 4 was evaluated. The results showed that Ag 3 PO 4 /CoFe 2 O 4 exhibited the best performance in the reduction of 4-nitrophenol (4-NP) and 2-nitrophenol (2-NP) and revealed 100% conversion into the corresponding amino derivatives within 24-46 min with rate constant equal to 0.0714 min À1 and 0.0329 min
À1, respectively.Moreover, due to the existence of the CoFe 2 O 4 , the Ag 3 PO 4 /CoFe 2 O 4 nanocomposite could be magnetically separated from the reaction mixture and reused without any change in structure.