“…The general composition, presented in Table 1, was determined by optical emission spectroscopy, ARL MA-310. Carbon and sulfur were determined as in [18] by combustion method using LECO CS-600 (CS 600 series, LECO Corporation, St. Joseph, Michigan, MI, USA) and nitrogen by LECO TC-500 (TC 500, RO 500, TN 500 series, LECO Corporation,St. Joseph, Michigan, MI, USA).…”