2020
DOI: 10.1016/j.jct.2019.105964
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Measurement of low-temperature heat capacity by relaxation technique: Calorimeter performance testing and heat capacity of benzo[b]fluoranthene, benzo[k]fluoranthene, and indeno[1,2,3-cd]pyrene

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Cited by 14 publications
(27 citation statements)
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“…Heat capacity of the Cu cup was subtracted from the total heat capacity using data recommended by Arblaster [16]. This technique was checked by measurement of compounds with reliable data obtained by adiabatic calorimetry (anthracene [17], l-asparagine [18], and glycine [19]) and uncertainty of results was found comparable to this reported previously [20] for samples encapsulated in Al DSC pans, i.e., the combined expanded uncertainty (0.95 level of confidence) of the heat capacity measurements is estimated to be…”
Section: Heat Capacity Measurementsmentioning
confidence: 98%
“…Heat capacity of the Cu cup was subtracted from the total heat capacity using data recommended by Arblaster [16]. This technique was checked by measurement of compounds with reliable data obtained by adiabatic calorimetry (anthracene [17], l-asparagine [18], and glycine [19]) and uncertainty of results was found comparable to this reported previously [20] for samples encapsulated in Al DSC pans, i.e., the combined expanded uncertainty (0.95 level of confidence) of the heat capacity measurements is estimated to be…”
Section: Heat Capacity Measurementsmentioning
confidence: 98%
“…However, a recent scan of the literature brought forth a number of further publications, which either confirmed previous data or even improved the conformance with prediction, but also enabled an extension of the applicability of the present GA approach. A number of new experimental C p data have been published for saturated and unsaturated hydrocarbons, especially for bicyclo [ [14], and adamantane [15]. In addition, further C p values have been found for the amines hexamethylenetetramine [15], tetra-N-phenylbenzidine and 4,4 -bis (N-carbazolyl)-1,1 -biphenyl [16], 1,3,5-triazine [17], the ethers 1,3,5-trioxane [17], diethylene glycol n-pentyl ether [18], triethylene glycol monopentyl ether [19] and diphenyl ether [20], several alcohols and aldehydes [21], derivatives of glycidol [22], carboxylic acids [23,24], aliphatic esters [24][25][26][27], benzoates [28], haloalkanes [29,30], haloaromatics [31,32], thio ethers, sulfones and sulfoxides [33,34], alkanolamines, [35][36][37] and nitriles [38] For several compounds, more recent publications have been found the following: 4-ethylmorpholine [39], methionine [40], theophylline, and caffeine [41], as well as for (-)-menthone, (+)-pulegone, and (-)-isopulegol [42].…”
Section: Sources Of Heat-capacity Datamentioning
confidence: 99%
“…The specific heat capacity of a sample is determined by measuring the thermal response to a change in heating conditions [ 35 ]. Uncertainty in the heat capacity obtained using PPMS was investigated recently in our laboratory [ 36 ]. Based on testing with several compounds [ 36 ], the combined expanded uncertainty (0.95 level of confidence) of the heat capacity measurements is estimated to be below 10 K, in the temperature range from 10 to 40 K and in the temperature range from 40 to 300 K.…”
Section: Methodsmentioning
confidence: 99%