Melamine supported magnetic iron oxide nanoparticles (Fe3O4@Mel) for spectrophotometric determination of malachite green in water samples and fish tissues

Mirzajani, Roya; Ahmadi, Shokufeh

doi:10.1016/j.jiec.2014.08.011

Cited by 46 publications

(4 citation statements)

References 41 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Among different types of IONP, Magnetite (Fe 3 O 4 ) nanoparticles are extensively used in magnetic separation, targeted drug delivery, magnetic resonance imaging, tissue engineering, bio-separation, magnetic hyperthermia and cell tracking (Mirzajani & Ahmadi, 2015; Thomas et al, 2015; Torres et al, 2010; Tudisco et al, 2015). Earlier research in vivo has demonstrated that Magnetite nanoparticles are comparatively benign due to their non-accumulating tendencies inside the vital organs.…”

Section: Introductionmentioning

confidence: 99%

Magnetically directed antioxidant and antimicrobial agent: synthesis and surface functionalization of magnetite with quercetin

Shah

Yehye

Chowdhury

et al. 2019

PeerJ

View full text Add to dashboard Cite

Oxidative stress can be reduced substantially using nanoantioxidant materials by tuning its surface morphological features up to a greater extent. The physiochemical, biological and optical properties of the nanoantioxidants can be altered by controlling their size and shape. In view of that, an appropriate synthesis technique should be adopted with optimization of the process variables. Properties of magnetite nanoparticles (IONP) can be tailored to upgrade the performance of biomedicine. Present research deals with the functionalization IONP using a hydrophobic agent of quercetin (Q). The application of quercetin will control its size using both the functionalization method including in-situ and post-synthesis technique. In in-situ techniques, the functionalized magnetite nanoparticles (IONP@Q) have average particles size 6 nm which are smaller than the magnetite (IONP) without functionalization. After post functionalization technique, the average particle size of magnetite IONP@Q2 determined was 11 nm. The nanoparticles also showed high saturation magnetization of about 51–59 emu/g. Before starting the experimental lab work, Prediction Activity Spectra of Substances (PASS) software was used to have a preliminary idea about the biological activities of Q. The antioxidant activity was carried out using 2, 2-diphenyl-1-picrylhydrazyl (DPPH) assay. The antibacterial studies were carried out using well diffusion method. The results obtained were well supported by the simulated results. Furthermore, the values of the half maximal inhibitory concentration (IC50) of the DPPH antioxidant assay were decreased using the functionalized one and it exhibited a 2–3 fold decreasing tendency than the unfunctionalized IONP. This exhibited that the functionalization process can easily enhance the free radical scavenging properties of IONPs up to three times. MIC values confirms that functionalized IONP have excellent antibacterial properties against the strains used (Staphylococcus aureus, Bacillus subtilis and Escherichia coli) and fungal strains (Aspergillus niger, Candida albicans, Trichoderma sp. and Saccharomyces cerevisiae). The findings of this research showed that the synthesized nanocomposite has combinatorial properties (magnetic, antioxidant and antimicrobial) which can be considered as a promising candidate for biomedical applications. It can be successfully used for the development of biomedicines which can be subsequently applied as antioxidant, anti-inflammatory, antimicrobial and anticancer agents.

show abstract

Section: Introductionmentioning

confidence: 99%

Magnetically directed antioxidant and antimicrobial agent: synthesis and surface functionalization of magnetite with quercetin

Shah

Yehye

Chowdhury

et al. 2019

PeerJ

View full text Add to dashboard Cite

show abstract

“…Not less than 80.0% extraction of MGD was observed with these effluent samples. The NACSAA and NACSAB-based methods developed in this investigation were compared with the reported literature (Zhang et al 2008;Arivoli et al 2009;Khattri & Singh 2009;Sekhar et al 2009;Saha et al 2010b;Tsai & Chen 2010;Parthasarathy et al 2011;Santhi et al 2011;Chieng et al 2014;Gautam et al 2015;Mirzajani & Ahmadi 2015) with respect to q e (mg/g) and pH (Table 6). It is inferred from the table that NACSAA (40.0 mg/g) and NACSAB (53.0 mg/g) have shown higher adsorption capacity than hitherto reported adsorbents in the literature.…”

Section: Applicationsmentioning

confidence: 99%

Statistical analysis on the removal of malachite green dye using active carbons of Achyranthes aspera and Allamanda blanchetii plants

Ravulapalli

Ravindhranath

2019

Water Practice and Technology

View full text Add to dashboard Cite

Activated carbons were prepared from the stem parts of Achyranthes aspera and Allamanda blanchetii plants and were investigated as adsorbents for the removal of malachite green dye from contaminated water. Various extraction conditions such as pH, initial concentration of dye, adsorbent dosage, temperature, agitation time and presence of co-ions were optimized for the maximum possible extraction of the dye. For analyzing the combined effect of these parameters on the removal efficiency of the adsorbents, statistical optimization modelling was adopted. The adsorbents developed were characterized and the adsorption abilities were observed to be 40.0 mg/g and 53.0 mg/g for the active carbons of Achyranthes aspera and Allamanda blanchetii plants respectively. The mechanism of adsorption was studied using various isotherm models and it was found that the Freundlich model describes well the adsorption process. Thermodynamic studies revealed the endothermic and spontaneous nature of physisorption. The kinetics of adsorption were well defined by the pseudo-second-order model. Desorption and regeneration studies of the spent adsorbents indicated that the percentage of extraction has not come down below 80.0% even after five regenerations for both the adsorbents. The validity of the methods developed are tested with real dye-polluted industrial effluent samples.

show abstract

“…After centrifugation, the upper layer was separated and the ethanol was evaporated. After addition of buffer and adjustment of pH, the volume was adjusted to 100 mL and the dyes were determined by the recommended procedure [31].…”

Section: Preparation Of Fish and Shrimp Muscle Samplesmentioning

confidence: 99%

Simultaneous preconcentration and determination of malachite green and fuchsine dyes in seafood and environmental water samples using nano-alumina-based molecular imprinted polymer solid-phase extraction

Mirzajani

Bagheban

2016

International Journal of Environmental Analytical Chemistry

Self Cite

View full text Add to dashboard Cite

Molecular imprinted polymer for determination of malachite green (MG) and fuchsine basic (FU) dyes by spectrophotometry has been used, to develop a novel simultaneous extraction and preconcentration method. Molecularly imprinted layer-coated nano-alumina (MIP@Nano-Al 2 O 3 ) as adsorbent was prepared by surface molecular imprinting technique, and characterised by FTIR spectroscopy, scanning electron microscopy, energy dispersive X-ray analysis (EDAX) and thermogravimetric analysis (TGA). The method is based on simultaneous extraction of MG and FU dyes from aqueous solution by using molecularly imprinted polymer and measuring the absorbance at 617 and 546 nm for MG and FU, respectively. Parameters which affect the extraction efficiency such as pH, volume of eluent and amount of adsorbent were investigated and optimised. Linear calibration curves were obtained in the range of 2-750 ng mL −1 for MG and 1-240 ng mL −1 for FU under optimum conditions. Detection limit based on three times the standard deviation of the blank (3S b ) was 0.655 and 0.245 ng mL −1 (n = 10) for MG and FU, respectively. The relative standard deviation (RSD) for 100 ng mL −1 of MG and FU was 2.35 and 3.06% (n = 7), respectively. The method was applied to the simultaneous determination of the dyes in different seafood and environmental water samples. ARTICLE HISTORY

show abstract

Melamine supported magnetic iron oxide nanoparticles (Fe3O4@Mel) for spectrophotometric determination of malachite green in water samples and fish tissues

Cited by 46 publications

References 41 publications

Magnetically directed antioxidant and antimicrobial agent: synthesis and surface functionalization of magnetite with quercetin

Magnetically directed antioxidant and antimicrobial agent: synthesis and surface functionalization of magnetite with quercetin

Statistical analysis on the removal of malachite green dye using active carbons of Achyranthes aspera and Allamanda blanchetii plants

Simultaneous preconcentration and determination of malachite green and fuchsine dyes in seafood and environmental water samples using nano-alumina-based molecular imprinted polymer solid-phase extraction

Contact Info

Product

Resources

About