Micro-strain, dislocation density and surface chemical state analysis of multication thin films

Jayaram, P.; Pradyumnan, P. P.; Karazhanov, Smagul

doi:10.1016/j.physb.2016.08.018

Cited by 25 publications

(2 citation statements)

References 26 publications

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“…As the temperature increases, the formation of a complex peak around the O1s peak is appreciated, with binding energies of Zn-O (∼530 eV) and Zn-OH (531.5 eV). This complex peak has been reported also by Jayaram, et al 45 for samples growth at very high temperature (1000 • C), explaining the increasing behavior of the Zn-O peak (∼530 eV) by the increasing of O H − ions. Thus, the possibility of the formation of Zn(OH) 2 is higher for higher temperatures while solely ZnO is mostly obtained for the low temperature of 25 • C, in agreement with the previous XRD results.…”

Section: Xrd Analysis-figuresupporting

confidence: 80%

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature

Rosado-Mendoza

Oliva-Avilés

Oliva

2017

ECS J. Solid State Sci. Technol.

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Zinc oxide (ZnO) and zinc hydroxide (Zn(OH)2) thin films were deposited by the chemical bath deposition onto glass substrates at temperatures of 25°C, 35°C and 45°C. The experimental conditions for the selective deposition of the films such as the concentration of the reagents, temperature, and pH of the chemical bath were determined from the predictions of the species distribution diagrams (SDDs) and solubility curves (SCs). SDDs and SCs were elaborated by considering the chemical reagents, temperature, and pH, and give information about the probability of formation of specific compounds. The reagents used were ZnSO4, KOH, and NH4NO3. The physicochemical of the synthesis of both ZnO and Zn(OH)2 films are proposed. X-ray photoelectron spectroscopy and X-ray diffraction indicate the presence of ZnO and/or Zn(OH)2 compounds, where the selective deposition of each material (or coexistence) is dependent on the bath temperature and pH. The crystalline structure was hexagonal (zincite) for ZnO and orthorhombic (wulfingite) for Zn(OH)2. The bandgap energy of the deposited films ranged from 3.32 to 3.51 eV. A better understanding of the selective deposition of specific compounds by controlling the experimental parameters represents an important step toward the fabrication of nanomaterials with tailored properties for a wide range of applications.

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Section: Xrd Analysis-figuresupporting

confidence: 80%

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature

Rosado-Mendoza

Oliva-Avilés

Oliva

2017

ECS J. Solid State Sci. Technol.

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“…1 . These peaks con rm the formation of TiO 2 /ZnO/ Fe 2 O 3 composites and the broad intense peaks are substantiating evidence for the growth of nano-sized grains, this speculation is established with the grain size calculations performed by Scherrer equation [12] [ The speci c surface area has a pronounced effect on photocatalytic activity. The BET results indicate that the presence of Zn 2+ and Fe 3+ ion has signi cantly in uenced the increase of the surface area of the samples.…”

Section: Structural Analysissupporting

confidence: 60%

Synthesis,Surface Morphology, Optical Properties and Photocatalyst Activities of TiO2/ZnO/Fe2O3 Nanocomposites.

Parambil¹,

V.M

Karazhanov

et al. 2020

Preprint

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The photocatalytic degradation of methylene blue in aqueous solutions is enhanced significantly by formulating multiphase TiO2/ZnO/Fe2O3 nanocomposites. The photocatalytic activity of unary TiO2, binary TiO2/ZnO, and ternary TiO2/ZnO/Fe2O3 compounds are compared and reported. Using TiO2/ZnO/Fe2O3, methylene blue degradation became rapid and the reaction followed first-order kinetics. The consequences of the phase transition, surface features, and optical properties are compared and elucidated. The reduced photoluminescence intensity and decreased optical band gap energy in tertiary compounds impose higher degradation of methylene blue under irradiation.

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Al–Ni Duplex Ion Implantation of Nickel Aluminum Bronze (NAB) to Improve the Corrosion Properties

Madhubala

Thillairajan

2022

Springer Proceedings in Materials

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Micro-strain, dislocation density and surface chemical state analysis of multication thin films

Cited by 25 publications

References 26 publications

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature

Synthesis,Surface Morphology, Optical Properties and Photocatalyst Activities of TiO2/ZnO/Fe2O3 Nanocomposites.

Al–Ni Duplex Ion Implantation of Nickel Aluminum Bronze (NAB) to Improve the Corrosion Properties

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Micro-strain, dislocation density and surface chemical state analysis of multication thin films

Cited by 25 publications

References 26 publications

Investigation of the Selective Growth of ZnO and Zn(OH)2Films Deposited by Chemical Bath Near Room Temperature

Investigation of the Selective Growth of ZnO and Zn(OH)2Films Deposited by Chemical Bath Near Room Temperature

Synthesis,Surface Morphology, Optical Properties and Photocatalyst Activities of TiO2/ZnO/Fe2O3 Nanocomposites.

Al–Ni Duplex Ion Implantation of Nickel Aluminum Bronze (NAB) to Improve the Corrosion Properties

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About

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature

Investigation of the Selective Growth of ZnO and Zn(OH)₂Films Deposited by Chemical Bath Near Room Temperature