Experimental research was carried out on the manufacturing of bio-coal briquettes from a blend of two different types of low-quality coal and biomass waste in the absence of coal carbonization, where the third blend of the material was fermented by adding a bio-activator solution before pressurizing the components into briquettes. The coal samples from Caringin-Garut Regency (BB-Garut) had a low calorific value and a high sulfur content (6.57 wt%), whereas the coal samples from Bayah-Lebak Regency (BB-Bayah) had a higher calorific value and a lower sulfur content (0.51 wt%). The biomass added to the coal blend is in the form of fermented cow dung (Bio-Kohe), and it had a calorific value of 4192 kcal/ kg and a total sulfur content of 1.56 wt%. The main objective of this study is to determine the total decrease in the sulfur content in a blend of coal and biomass in which a fermentation process was carried out using a bio-activator for 24 h. The used bio-activator was made from GarantÒ (1:40) ? molasses 1 wt%/vol, and its used amount was 0.2 L/kg. Also, the total sulfur content in the blend was 1.00 wt%-1.14 wt%, which fulfills the necessary quality requirements for non-carbonized bio-coal briquettes. The pyritic and sulfate content in the raw coal was dominant, and the organic sulfur, when fermented with GarantÒ, was found to be less in the produced bio-coal briquettes by 38%-58%.