2008
DOI: 10.1556/jpc.21.2008.4.3
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Microwave assisted thin-layer chromatography — an improved separation technique

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Cited by 6 publications
(4 citation statements)
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“…Taking into account the interaction of MW radiation with matter several attempts have been published trying to use MW for improving the separation of compounds in chromatography . In TLC a perpendicular arrangement of the MW field relative to the TLC plate allowed obtaining a considerable improvement in the separation of dyes and pesticides compared with separation under usual conditions. A different application was the design of a MW GC oven in which only the column was heated because the column contains the only appropriate MW absorbing material.…”
Section: Introductionmentioning
confidence: 99%
“…Taking into account the interaction of MW radiation with matter several attempts have been published trying to use MW for improving the separation of compounds in chromatography . In TLC a perpendicular arrangement of the MW field relative to the TLC plate allowed obtaining a considerable improvement in the separation of dyes and pesticides compared with separation under usual conditions. A different application was the design of a MW GC oven in which only the column was heated because the column contains the only appropriate MW absorbing material.…”
Section: Introductionmentioning
confidence: 99%
“…OPLC is performed in a compact set-up. Soran et al (73) used electromagnetic waves to improve chromatographic interactions between the stationary phase and mobile phase. Dzido et al (74) checked the effect of temperature on the behavior of aromatic hydrocarbons using reversed-phase TLC in the range of 285 8K through 331 8K.…”
Section: Discussionmentioning
confidence: 99%
“…The vast majority of TLC analyses are carried out by a single capillary flow ascending development in a mobile phase vapor saturated large volume chamber (N-chamber) or Camag twin trough chamber (44) Methods of obtaining optimum separations for circular and linear TLC by applying focusing liquids to the initial zone were described (91). Application of a microwave field arranged perpendicular to the TLC plate resulted in improved separations (92). A simple temperature controlled horizontal chamber for nonforced flow microplanar NP and RP TLC was described for isothermal or gradient developments from -20 to 80 °C in 5-20 min using 0.3-1.0 mL of mobile phase and applied to separations of cyclodextrins, fullerines, and steroids (93).…”
Section: Apparatus and Techniquesmentioning
confidence: 99%