The Y 3 MgAl 3 SiO 12 ceramics with pure phase were successfully synthesized by solid-state sintering reaction method for the first time. Their microwave dielectric properties were investigated as a function of sintering temperature. Their microstructure characteristics and ionic occupation sites of tetrahedral and octahedral units were characterized and analyzed by SEM& energy dispersive spectrometer (EDS) and Rietveld refinement of X-ray powder diffraction data. Crystal 1,2 Up to now, many materials with high quality factor (Qf values) to depress energy loss, low dielectric constant (e r ) to reduce the delay time of electronic signal transmission, and ideal near zero temperature coefficient of resonant frequency (s f ) for working frequency stability have been reported and used as resonators, filters, dielectric antennas, dielectric guided wave circuits, and other microwave components. To solve these problems, various kinds of silicate ceramic materials, such as forsterite Mg 2 SiO 4, 5 willemite