“…Fusion in a glass tube on the macro scale was described by Elving and Ligett using sodium metal (16) and by Silvey and Cady using potassium (42). Kainz and Scholler (21) adapted the procedure to microanalysis. The drawback of the sealed glass tube technique is the requirement of evacuation and glass blowing facility.…”
Determination of fluorine in organic microanalysis has become increasingly important because of the large number and variety of organic fluoro compounds being synthesized.
“…Fusion in a glass tube on the macro scale was described by Elving and Ligett using sodium metal (16) and by Silvey and Cady using potassium (42). Kainz and Scholler (21) adapted the procedure to microanalysis. The drawback of the sealed glass tube technique is the requirement of evacuation and glass blowing facility.…”
Determination of fluorine in organic microanalysis has become increasingly important because of the large number and variety of organic fluoro compounds being synthesized.
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