MIL-53(Al)/Fe2O3 nanocomposite for solid-phase microextraction of organophosphorus pesticides followed by GC-MS analysis

Moinfar, Soleyman; Khodayari, Ali; Sohrabnezhad, Sh.; Aghaei, Ali; Jamil, Lazgin A.

doi:10.1007/s00604-020-04621-z

Cited by 40 publications

(8 citation statements)

References 39 publications

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“…The modern method of separating and identifying residual amounts of pesticides in grapes also requires a good foundation in the form of detectors. MS is a very sensitive analyzer [ 33 , 50 ] to determine organophosphate pesticides, but this does not exclude the fact that it remains an excellent analyzer for other classes of pesticides. Photodiode array detector (PDA) remains a specific analyzer [ 36 ] to determine peritroidal pesticides in grapes.…”

Section: Instrumental Detection Methodsmentioning

confidence: 99%

“…This is explained by the fact that pesticides of this class are chemicals that effectively control and destroy harmful microorganisms and are also fungicides for a wide range of uses with low toxicity [ 20 , 25 ]. After the triazole class fungicides, organophosphate pesticides are the next commonly known and used (~14%), which effectively fight against the pests of the grapes [ 32 , 33 , 34 , 35 ]. A widespread pesticide used for the cultivation of grape is multiclass pesticides, which involve 13% of other pesticides with different biological activities such as fungicides, acaricides, insecticides, herbicides, and plant growth regulators [ 9 , 22 ].…”

Section: Introductionmentioning

confidence: 99%

“…Environmental conditions, such as sunlight, temperature and humidity, play an essential role in the kinetic and dynamic behaviors of pesticides [ 14 , 17 , 18 ]. The use of separate classes of pesticides helps to solve problems of various kinds; for example, one of the commonly used pesticides is pyrethroids [ 18 , 25 , 33 ]. Pyrethroids are a synthetic class of pesticides derived from natural chrysanthemum esters.…”

Section: Introductionmentioning

confidence: 99%

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Modern Analytical Methods for the Analysis of Pesticides in Grapes: A Review

Syrgabek

Alimzhanova

2022

Foods

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Currently, research on the determination of pesticides in food products is very popular. Information obtained from research conducted so far mainly concerns the development of a methodology to determine the content of pesticides in food products. However, they do not describe the content of the pesticide used in viticulture in the resulting product. Over the past decade, this study has examined analytical methodologies for assessing pesticide residues in grapes. Scopus, Web of Science, Science Direct, PubMed, and Springer databases were searched for relevant publications. The phrases “pesticides” and “grapes” and their combinations were used to search for articles. The titles and annotations of the extracted articles have been read and studied to ensure that they meet the review criteria. The selected articles were used to compile a systematic review based on scientific research and reliable sources. The need to study the detection of pesticide residues in grapes using advanced analytical methods is confirmed by our systematic review. This review also highlights modern methods of sample preparation, such as QuEChERS, SPME, PLE, dLLME, and ADLL-ME, as well as the most used methods of separation and identification of pesticides in grapes. An overview of the countries where residual grape pesticide amounts are most studied is presented, along with the data on commonly used pesticides to control pests and diseases in grape cultivation. Finally, future possibilities and trends in the analysis of pesticide residues in grapes are discussed by various analytical methods.

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Section: Instrumental Detection Methodsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

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Modern Analytical Methods for the Analysis of Pesticides in Grapes: A Review

Syrgabek

Alimzhanova

2022

Foods

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“…Furthermore, the MIL‐53(Al)/Fe 2 O 3 composite was employed by Moinfar et al. as an excellent adsorbent for coating SPME fibers to extract organophosphorus compounds (OPPs) from the river water, tea samples, and juices [105] . Similarly, Pang et al.…”

Section: Environmental Analysis Applicationsmentioning

confidence: 99%

Electrochemical Synthesis Methods of Metal‐Organic Frameworks and Their Environmental Analysis Applications: A Review

Ren

Wei

2022

ChemElectroChem

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ing new MOFs and developing novel eco-friendly electrochemical synthesis methods for MOFs' application in environmental analysis. Moreover, the applications of MOFs in environmental analysis field in recent years were comprehensively illustrated and the advantages and disadvantages of electrochemical synthesis methods to prepare MOFs as environmental analytical nanomaterials were evaluated. Finally, some suggestions for the optimization of electrochemical synthesis methods for MOFs and their future opportunities in environmental analytical applications were proposed.

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“…The purpose of the sample preparation step is to decrease or eliminate matrix interferences, enrich the analytes, and transfer the analytes to an analyzable phase with the analytical system [4, 5]. The sample preparation process for pesticide residue analysis in water mostly includes SPE [6, 7], dispersive liquid‐liquid micro‐extraction [8], SPME [9], and magnetic SPE (MSPE) [10, 11]. Some problems with the SPE procedure are consuming a high volume of organic solvents, and being labor‐intensive and tedious [12].…”

Section: Introductionmentioning

confidence: 99%

Magnetic solid‐phase extraction of organophosphorus pesticides from apple juice and environmental water samples using magnetic graphene oxide coated with poly(2‐aminoterephthalic acid‐co‐aniline) nanocomposite as a sorbent

Nasiri

Ahmadzadeh

Amiri

2022

J of Separation Science

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An effective magnetic solid-phase extraction method was proposed using magnetic graphene oxide coated with poly(2-aminoterephthalic acid-co-aniline) as a sorbent for preconcentration and extraction of organophosphorus pesticides from environmental water and apple juice samples, and determined using the gas chromatography-mass spectrometry analysis. To approve the successful synthesis of the magnetic nanocomposite, the prepared sorbent was characterized by field emission scanning electron microscopy, X-ray diffraction, vibrating sample magnetometer, and Fourier transforms infrared techniques. The main parameters affecting the extraction efficiency were considered and studied to afford an optimized procedure. Systematic method validation verified its suitable recoveries (89.4-107.3%), and precision (relative standard deviations < 6.8%). The method showed a wide linear dynamic range (0.04-700 ng/mL) with low limits of detection (0.01-0.06 ng/mL) and quantification (0.04-0.21 ng/mL). This method presented good potential and great sensitivity for the pesticides determination.

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MIL-53(Al)/Fe2O3 nanocomposite for solid-phase microextraction of organophosphorus pesticides followed by GC-MS analysis

Cited by 40 publications

References 39 publications

Modern Analytical Methods for the Analysis of Pesticides in Grapes: A Review

Modern Analytical Methods for the Analysis of Pesticides in Grapes: A Review

Electrochemical Synthesis Methods of Metal‐Organic Frameworks and Their Environmental Analysis Applications: A Review

Magnetic solid‐phase extraction of organophosphorus pesticides from apple juice and environmental water samples using magnetic graphene oxide coated with poly(2‐aminoterephthalic acid‐co‐aniline) nanocomposite as a sorbent

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